Characterization of Pousão Pigments and Extenders by Micro-X-ray Diffractometry and Infrared and Raman Microspectroscopy

Andreia M. Correia · Maria Jovita Oliveira · Robin J. H. Clark · M.L. Duarte

54 citations0/0 files storedAnalytical Chemistry

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Cultural Heritage Materials Analysis Historical Art and Architecture Studies Mineralogy and Gemology Studies

Abstract

Seventeen samples from paintings by the distinguished 19th century Portuguese painter, Henrique Pousão, were characterized by micro-X-ray diffractometry and infrared and Raman microspectroscopy. The main advantages and limitations of each technique for pigment identification are outlined, revealing the need for the use of complementary techniques. Pousão's palette is discussed.

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References

2001Library of FT-Raman spectra of pigments, minerals, pigment media and varnishes, and supplement to existing library of Raman spectra of pigments with visible excitation 2003Catalogue of 45 reference Raman spectra of minerals concerning research in art history or archaeology, especially on corroded metals and coloured glass 2001Pigment identification in paintings employing laser induced breakdown spectroscopy and Raman microscopy 1996Characterization of Pararealgar and Other Light-Induced Transformation Products from Realgar by Raman Microspectroscopy 2000Pigment Identification in Painted Artworks: A Dual Analytical Approach Employing Laser-Induced Breakdown Spectroscopy and Raman Microscopy 2007Pigment study by Raman microscopy of 23 paintings by the Portuguese artist Henrique Pousão (1859–1884)2000Microscopic and imaging Raman scattering study of PbS and its photo-oxidation products 2003Spectroscopic investigation of yellow majolica glazes

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2010Raman spectroscopic discrimination of pigments and tempera paint model samples by principal component analysis on first‐derivative spectra 2010Studies of wall painting fragments from Kaiping Diaolou by SEM/EDX, micro Raman and FT-IR spectroscopy 2008Innovative Analytical Methodology Combining Micro-X-Ray Diffraction, Scanning Electron Microscopy-Based Mineral Maps, and Diffuse Reflectance Infrared Fourier Transform Spectroscopy to Characterize Archeological Artifacts

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