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A method is described for the analysis of archaeological rock artefacts which provides major and trace element data. Wavelength‐dispersive X‐ray fluorescence (WDXRF) analysis of 2:1 fusion beads permits the accurate and precise measurement of a wide range of elements. Accuracy and precision are nominally 1‐5% for elements having concentrations above 3 times the detection limit. The method requires a much smaller sample size than conventional WDXRF procedures and has been successfully used to characterise early millstones; a number of other applications in archaeology are suggested here.
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