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Validation of quantitative NMR

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References

2004Quality Systems—Medical Devices—Particular Requirements for the Application of ISO 90012,696 cited
1995Guide to the Expression of Uncertainty in Measurement815 cited

Cited by

2012Determination of standard sample purity using the high-precision 1H-NMR process86 cited
2008A new traceability scheme for the development of international system-traceable persistent organic pollutant reference materials by quantitative nuclear magnetic resonance83 cited
2013Using high-performance quantitative NMR (HP-qNMR®) for certifying traceable and highly accurate purity values of organic reference materials with uncertainties <0.1 %79 cited
2018A New Realization of SI for Organic Chemical Measurement: NIST PS1 Primary Standard for Quantitative NMR (Benzoic Acid)62 cited
2013Using high-performance 1H NMR (HP-qNMR®) for the certification of organic reference materials under accreditation guidelines—Describing the overall process with focus on homogeneity and stability assessment54 cited
2023Methods for the SI-traceable value assignment of the purity of organic compounds (IUPAC Technical Report)53 cited
2019Development and validation of a suite of standards for the purity assignment of organic compounds by quantitative NMR spectroscopy44 cited
2006Purity assessment problem in quantitative NMR—impurity resonance overlaps with monitor signal multiplets from stereoisomers41 cited
2011Efficient production of reference materials of hazardous organics using smart calibration by nuclear magnetic resonance35 cited
2014Purity assessment of organic calibration standards using a combination of quantitative NMR and mass balance

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34 cited

2014Bias and Uncertainty in Non-Ideal qNMR Analysis30 cited

2015Metrological approaches to organic chemical purity: primary reference materials for vitamin D metabolites24 cited

2014Establishment of the purity values of carbohydrate certified reference materials using quantitative nuclear magnetic resonance and mass balance approach24 cited

2016Chemical purity using quantitative1H-nuclear magnetic resonance: a hierarchical Bayesian approach for traceable calibrations23 cited

2014Quantitative NMR spectroscopy for accurate purity determination of amino acids, and uncertainty evaluation for different signals23 cited

2019The role of the CCQM OAWG in providing SI traceable calibrators for organic chemical measurements21 cited