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The grounds of nine fifteenth-sixteenth century panels of the Castilian School were studied. The material used was gypsum in all cases. Examination as backscattered electron images by scanning electron microscopy showed the different morphologies of the materials used in the gesso grosso and gesso sottile layers. Energy dispersive X-ray analysis (SEM-EDX) was used to determine the purity of the gypsum and provide preliminary data on the nature of the associated minerals (dolomite, calcite and various silicates).
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