Identification par microscopie Raman des tessons et pigments de glaçures de céramiques de L'Ifriqiya (Dougga, XI-XVIIIèmes siècles)

Philippe Colomban · Gérard Sagon · Adnan Louhichi · Housam Binous · Naceur Ayed

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Cultural Heritage Materials Analysis Mineralogy and Gemology Studies Building materials and conservation

Abstract

Raman (micro)spectrometry is used as a technique for the understanding and identification of the fabrication technology of ancient faience and glazed terra cotta from Dougga, north-west of Tunisia. Studied samples are assigned to zirides (XI-XIIth), almohades (XIII-XVth), hafsides and ottomane (XVII-XVIIth) periodes. Cassitérite (SnO2) white, (Pb2Sb,O7) Naples yellow, black and (Fe/Mn ?) brown spinels, haematite (Fe2O3) black and unassigned blue pigment have been characterized. Green colour results from glaze doping (by Cu ?), except for recent samples where woUastonite phase, easely colored in green by chrome, is found. A cassiterite-free overglaze is often present. Cassitérite amounts appear too low in ancient samples to really opacify the enamel.

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1996De l'origine du cobalt : du verre à la céramique 1992De l'origine du cobalt dans les verres

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