Synthesis and Analysis by Liquid Chromatography-Mass Spectrometry of a Mauveine Composition Similar to Museum-Stored Mauveine

Michael John Plater · Andrea Raab

10 citations0/0 files storedJournal of Chemical Research

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Cultural Heritage Materials Analysis Synthesis and Properties of Aromatic Compounds Dye analysis and toxicity

Abstract

Our proposal that museum-stored mauveine was made by a modified method compared to mauveine made by the William Henry Perkin patented method of 1856 is exemplified. An improved method of purification allows greater resolution and separation of the different mauveine chromophores. Liquid chromatography-mass spectrometry charts for museum-stored mauveine are compared to the new mauveine reported here. The formation of deprotected mauveine chromophores and N-tert- butylated mauveine chromophores is discussed.

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2003Research Universities and Local Economic Development: Lessons from the History of the Johns Hopkins University 2008A Study in Mauve: Unveiling Perkin's Dye in Historic Samples 2017Reconstructing the historical synthesis of mauveine from Perkin and Caro: procedure and details 2014Perkin’s and Caro’s Mauveine in Queen Victoria’s Lilac Postage Stamps: A Chemical Analysis

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2020Liquid chromatography–mass spectrometry analysis of cationic aniline dyes from the Technical University of Dresden Historical Collection of Dyes

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