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In this paper multi-spectroscopic techniques for characterization of ancient potsherds excavated from different Neolithic sites (Esh-shaheinab, Kadero and Jebel-Um-Marahi), Sudan were reported. The experimental data inform us to the both elemental and mineralogical composition of the potsherds. Mineralogical composition of ancient pottery has been studied by both FTIR and XRD approaches. Further, studies by Thermogravimetric analysis (TGA) to indicate the firing temperature from typical thermal reaction in potsherds samples. Scanning Electron Microscopy (SEM) coupled with an Energy Dispersive Spectrometer (EDS) was used to study the internal morphology and chemical composition of the pottery.
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