Identification of nineteenth century blue and green pigments by in situ x‐ray fluorescence and micro‐Raman spectroscopy

Francesca Rosi · Costanza Miliani · Ilaria Borgia · Brunetto Giovanni Brunetti · Antonio Sgamellotti

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Cultural Heritage Materials Analysis Historical Art and Architecture Studies Mineralogy and Gemology Studies

Abstract

Abstract A mural painting by the innovative Italian miniaturist Napoleone Verga (1833–1918) was studied by a model protocol that combines an in situ non‐destructive technique with laboratory micro‐destructive vibrational investigations. The experimental procedure allowed us to acquire detailed information not only on Verga's palette and painting technique but also on undocumented retouches, using a very restricted number of samples. Copyright © 2004 John Wiley & Sons, Ltd.

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References

2001Library of FT-Raman spectra of pigments, minerals, pigment media and varnishes, and supplement to existing library of Raman spectra of pigments with visible excitation 2000Analysis with micro-Raman spectroscopy of natural organic binding media and varnishes used in art 2002Pigment identification by spectroscopic means: an arts/science interface 2001Pigment identification in paintings employing laser induced breakdown spectroscopy and Raman microscopy 2002An extensive non‐destructive and micro‐spectroscopic study of two post‐Byzantine overpainted icons of the 16th century 2000Comparative pigment analysis of six modern Egyptian papyri and an authentic one of the 13th century BC by Raman microscopy and other techniques

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2011The use of a multi-method approach to identify the pigments in the 12th century manuscript Liber Floridus 2006Non-invasive and non-destructive micro-XRF and micro-Raman analysis of a decorative wallpaper from the beginning of the 19th century 2009In situ investigations of vault paintings in the Antwerp cathedral 2010Multivariate chemical mapping of pigments and binders in easel painting cross-sections by micro IR reflection spectroscopy 2006On the use of photobleaching to reduce fluorescence background in Raman spectroscopy to improve the reliability of pigment identification on painted textiles

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