GC‐MS Characterisation and Identification of Natural Terpenic Resins Employed in Works of Art

Giampaolo Cartoni · Mario Vincenzo Russo · Francesca Romana Spinelli · Fabio Talarico

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Cultural Heritage Materials Analysis Polymer Synthesis and Characterization Conservation Techniques and Studies

Abstract

Natural resins were frequently employed in the past as adhesives or as components of oleo-resinous media in paintings. The identification of vegetable resins is still an open problem. The aim of this paper is to analyse by GC-MS some vegetable resins frequently employed in paintings, such as Venice turpentine, dammar, copal, elemi, in order to identify their main components in samples both raw and aged. Some molecules are proposed as chemical markers to identify these natural resins. Two samples scraped off from XV and XVII century paintings were used to test the reliability of proposed method.

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References

1988The Organic Chemistry of Museum Objects 1977NATURAL RESINS OF ART AND ARCHAEOLOGY THEIR SOURCES, CHEMISTRY, AND IDENTIFICATION 2000Mass spectrometric methodology for the analysis of highly oxidized diterpenoid acids in Old Master paintings 1998Comparative chromatographic and mass-spectrometric studies of triterpenoid varnishes: fresh material and aged samples from paintings 1999Molecular studies of fresh and aged triterpenoid varnishes 2002Identification of non-cross-linked compounds in methanolic extracts of cured and aged linseed oil-based paint films using gas chromatography–mass spectrometry

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